Thomas B. Jones
Professor of Electrical Engineering
Ph.D., Massachusetts Institute of Technology, 1970
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Laser Target Fabrication using Microfluidics   Publications

In close collaboration with the Laboratory for Laser Energetics, we are exploiting electrowetting and liquid dielectrophoresis to fabricate and process targets for laser-driven inertial fusion. The three main thrusts are (i) electric field-mediated droplet centering; (ii) assembly line formation of double-emulsion droplets; (iii) manipulation & metering of cryogenic deuterium for target fueling.

Forming Concentric Double-Emulsion Droplets      Click images to view video

             

The videos above demonstrate use of a uniform AC electric field to center one liquid droplet inside another. One application is for highly concentric double-emulsion droplets to form polymer foam shells for laser targets. A fundamental requirement for centering is that the relative dielectric constant of the suspending liquid is lower than that of the outer shell. For 3 to 6 mm diameter droplets, centering occurs in ~60 seconds, with E ~ 10E4 V/m. A stronger field yields more rapid centering at the expense of increased ellipsoidal distortion. The required AC frequency depends on the electrical conductivity of the outer shell and its thickness. For the polymer chemistries of interest in foam shell fabrication, f ~ 20 MHz.

DEP Microactuation & Droplet Dispensing   Publications

We are investigating microfluidic schemes based on dielectrophoretic (DEP) and electrowetting-based (EWOD) for applications in the laboratory-on-a-chip. Principal efforts have been devoted to liquid manipulation and droplet dispensing in open geometries using non-uniform AC electric fields created by simple, co-planar electrodes patterned on a substrate. Such microfluidic systems are very fast; typically ~10 cm/sec, though ~50 cm/sec have been observed. Dispensing of linear arrays of uniformly sized droplets from hundreds of nanoliters down to tens of picoliters has been demonstrated. Scale-up to large 30x30 droplet arrays is possible. Recent work involved developing a smart system employing optical sensing and feedback to control the droplet dispenser.

      

The videos above shows various parallel-plate microfluidic structures patterned on transparent, InSn-oxide coated glass substrates. The liquid is DI water, the AC voltage frequency = ~100 kHz, and the applied voltage is typically ~200 V-rms. The view is through the transparent electrodes. The spiral structure on the right (electrode spacing = 100 microns & width = 200 microns) nicely visualizes the largely uncoupled roles of capillarity and liquid DEP in such microfluidic systems. With voltage on, the liquid is drawn along the narrow (transparent) electrodes. It is best not to think of this as a pumping mechanism, but rather an electric field coupled hydrostatic equilibrium, because the liquid stops when it gets to the end. During this motion, capillarity locally controls the liquid meniscus between the parallel, transparent electrodes; it is the DEP force due to the non-uniform E field that contains the liquid. When the voltage is removed and the electrical force gone, wetting causes the liquid to spread into the spaces between the electrodes, quickly filling the entire structure.

Basics of coplanar DEP microactuation      Click on image to view video

             

You may download a PDF file of the above (left) video showing operation of a DEP micronsiphon. When 60 kHz voltage is applied to the parallel co-planar strip electrodes, a narrow finger of water (de-ionized) emerges from the large ~10 microliter droplet at lower left, travels quickly along the 100 micron gap between them, turns two corners and then stops at the end of the structure. Note that this mechanism is not true pumping, but better thought of as a force induced by the non-uniform electric field and some akin to capillary action.

Capillary instability divides the finger into uniform droplets when voltage is removed. Placing a 45 degree angle mirror beside the electrodes facilitates simultaneous observation of the motion of the finger from above and from a low angle. The video at the above right reveals considerable information about the finger dynamics and shows the droplet formation when the voltage is removed.

The video at the right shows a two-stage droplet dispenser using four individually addressable electrodes. When voltage is first applied, an intermediate droplet of volume ~80 nanoliters collects at the upper left. Next, the electrode connections are changed, and rf voltage is again applied. Three separate droplets, each ~7 nanoliters, form rapidly in line and to the right of the intermediate droplet. The volume of the initial droplet at lower left, dispensed by a micropipette, is ~10 microliters.

Precision droplet dispensing      Click on image to view video

                

DEP can be used to dispense large numbers of very small droplets very rapidly from a single larger parent deposited manually with a micropipette. CLICK HERE to see an SEM and photomicrograph of a structure (R. Ahmed) that produced an array of 21 droplets of volume ~13 picoliter each. The three-electrode structure shown in the video at the left just above (R. Ahmed) operates by (i) filling the entire length of the electrodes with liquid, (ii) trapping the static liquid rivulet to the left of the T junction, and (iii) forming droplets at each bump by removal of the voltage. The video at the right, obtained by K. L. Wang, shows a similar structure fabricated on a <100> Si wafer.

Other interesting phenomena      Click on image to view video


In the video clip just above, ethylene glycol was actuated on strip electrodes in an insulating mineral oil bath. The relative interfacial tension between these two liquids is quite low. As a result, when voltage is removed the finger retracts back into the parent droplet to the left without forming droplets.
The siphon and two-stage droplet generator videos above were taken in 2000 by M. Gunji at Kyoto University.

Electromechanics of Liquids   Publications

We have investigated the hydrostatics and dynamics of liquids under the influence of variable frequency electric fields. EWOD and DEP liquid microactuation are, respectively, the low and high frequency limits of the electromechanical response of conductive, dielectric liquids. A simple RC circuit model successfully predicts these limits and the critical frequency that deliniates them. It may be shown that changes to the contact angle are not responsible for the motions exploited in microfluidic applications. CLICK HERE to download an updated lecture presentation (2007) that argues the case for an interpretation of EWOD as an electromechanical phenomenon.

Transient Motion      Click images to view video

Transient E-field driven microfluidic flows have been investigated intensively at Rochester. One important finding is that for aqueous liquids the so-called dynamic frictional force per unit length of the contact line seems to dominate viscous wall shear.


            
Surface Waves      Click images to view video

We are also studying the effects of AC time-varying electric fields upon contact angle and displacement using the classic experimental geometry of Pellat: parallel, vertical electrodes dipped into liquid. The high-speed videos above (taken by K-L. Wang) show the motion of DI water when AC voltage is suddenly applied to Parylene-coated electrodes. The liquid rises rapidly to approach the static equilibrium height. The applied frequency is 2 kHz for the video at the left and 100 Hz for the one at the right. Some interesting surface dynamics, most evident at lower frequencies, are revealed in the videos below.


              

In these four videos, the upward direction is to the left. The surface waves motion depends strongly on the frequency of the applied voltage. At DC, no sloshing motion is evident. For AC, strong surface vibrations and sloshing are evident. The sloshing is presumably due to parametric EHD surface instability. At an electrode spacing of ~2 mm, virtually all surface wave dynamics are suppressed above ~1 kHz. Furthermore, at 10 kHz the contact angle is ~90 degrees and the surface is almost flat.

Over the years, our research has been supported by the National Science Foundation (USA), the Japan Society for the Promotion of Science, the National Institutes of Health, the Center for Future Health (Univ. of Rochester), the Infotonics Technology Center, Inc., the Engineering and Physical Science Research Council (UK), NexPress Solutions, Inc., the Center for Electronic Imaging Science (Univ. of Rochester), Corning, Inc., the Laboratory for Laser Energetics (Univ. of Rochester), General Atomics, Eastman Kodak, Inc., and Cypress Semiconductors, Inc.

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Papers on E-field Induced Droplet Centering for Laser Target Fabrication


Papers on DEP Microactuation & Electrowetting


Microfluidics Patents


Papers on Ink Jet Physics


Papers on Electromechanics of Liquids


For J. R. Melcher's notes concerning electrical forces on dielectrics, CLICK HERE.

Books


Other research & educational activities

Electromechanics of Particles, Biological Dielectrophoresis, Levitation

Lecture Demonstrations on Electrostatics

On-line Interactive Nomograms

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Last modified on Friday, 27-Apr-2012 08:42:06 EDT